epa method 7471

10. The information contained in this method is provided by EPA as guidance to be used by the analyst and the regulated community in making judgments necessary to generate results that meet the data quality objectives for the intended application. %PDF-1.3 EPA Method 200.7 uses ICP-OES for regulatory compliance for drinking water analysis. Method 7471B: Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique), part of Test Methods for Evaluating Solid Waste, Physical/Chemical Methods (PDF) (11 pp, 1 MB, February 2007) Contact Us to ask a question, provide feedback, or report a problem. Laboratory Method … Our HotBlock manuals come with adapted versions of several EPA methods including 200.2, 200.7, 200.8, 245.1, 7470, 7471, 365.2, 3050B, and NIOSH method 7303. An official website of the United States government. Methods for Chemical Analysis of Water and Wastes, EPA-600/4-82-055, December 1982, Method 213.1. EPA 3050B: EPA 7470: EPA 7471: Don't see your test method listed? Primarily for the purpose of monitoring for mercury levels in fish and in support of consumption advisories, many environmental laboratories routinely utilize a common testing method, EPA Method 7471A: Mercury in Solid or Semisolid Waste(EPA 7471), for the preparation and analyses of biota samples for total mercury concentrations. 2, EPA Contract No. The information contained in this method is provided by EPA as guidance to be used by the analyst and the regulated community in making judgments necessary to generate results that meet the data quality objectives for the intended application. See EPA's PDF page to learn more. endobj 6000 Series. Additionally, EPA approved Method 1631 Revision E in 2002. The only thing to be aware of is differences in volume. 8.0 QUALITY CONTROL 8.1 See Section 8.0 of Method 7000. Methodologies include NELAP approved EPA Method 200.7, EPA SW-846 Method 6010 for ICP metals and EPA Method 245.1, EPA SW-846 Method 7470/7471 for Mercury analyses. Decomposition temperature: Not available. 2.2 This method uses cold-vapor atomic absorption and is based on the absorption of radiation at the 253.7-nm wavelength by mercury vapor. Validated Methods. 1000 Series. 11.1 (in the EMMC format) directs the user to weigh out 0.5 to 0.6 g of a well-homogenized sample. You can email us at info@envexp.com. 2. EPA’s Selected Analytical Methods for Environmental Remediation and Recovery (SAM) lists this method for preparation and/or analysis of solid and wipe samples for mercury, mercuric chloride (analyzed as total mercury), and methoxyethylmercuric acetate (analyzed as total mercury). Main menu . Screening Level 14 (µg/kg dry weight) [Minimum Detection Limit must be lower]: Total polychlorinated biphenyls (PCB) Footnote 15 Footnote 16 MA400-BPC 1.0 or EPA 1668C 17: method and/or lab dependent: 100: Total polycyclic aromatic hydrocarbons (PAH) Footnote 15 Footnote 18 EPA 8270C 1 0 obj See EPA’s About PDF page to learn more. If you are Product name: LOCTITE SF 7471 PRIMER known as LOCTITE® 7471™ Primer LOCQUIC® Page 4 of 6 Solubility in water: Not available. Gaskill, A., Compilation and Evaluation of RCRA Method Performance Data, Work Assignment No. If this dissolution procedure is not sufficient to dissolve a specific matrix type or sample, then this method is not applicable for that matrix. Method 1631E has a quantitation level of 0.5 ppt, making it 400 times more sensitive than Methods 245.1 and 245.2. Do you have a specification sheet available? 9.2 The performance characteristics for an aqueous sample free of interferences are: Optimum concentration range: 5-100 … Utilizing Cold Vapor Atomic Absorption (CVAA) technology, total mercury analysis is suitable for a variety of matrices including waters, soils, sediments and wastes. You may need a PDF reader to view some of the files on this page. Partition coefficient (n-octanol/water): Not available. ���0��i�)~�Ε ���%���]"h3����g�s�C�x�u ��*�zܜd�F}(oٰ̾���x�5�e���a�@,)��IP\? See EPA’s, Selected Analytical Methods for Environmental Remediation and Recovery (SAM), Method 7471B: Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique), part of Test Methods for Evaluating Solid Waste, Physical/Chemical Methods (PDF), Sample Collection Information Documents (SCIDs), Sample Collection Procedures and Strategies. 7000 Series. Method … EPA Method 7471B (SW-846): Mercury in Solid or Semisolid Wastes (Manual Cold-Vapor Technique) This document is included in Selected Analytical Methods for Environmental Remediation and … Aqueous samples are digested with sulfuric acid, nitric acid, potassium permanganate, and potassium persulfate in order to oxidize the organo-mercury compounds to the mercuric ion. The quantitation limit will depend on the volume of sample used to trap the mercury by the use of gold. 3000 Series. sand, silica gel, acid binder, universal binder, sawdust). 0010 - 0100 Series. All of the documents found in the Third Edition of SW-846, as updated by Updates I, II, IIA, IIB, III, IIIA, IIIB, IVA and IVB are located at this site. Organics: Analytical Method Footnote 12: Target 13 Detection Limit (mg/kg dry weight). 4000 Series . The heat content (higher heating value, HHV), as well as, moisture, ash, carbon, hydrogen, oxygen, nitrogen, and sulfur contents of both the firelogs and their combustion residues were determined by proximate/ultimate analyses. The method can also be used for analysis of other matrices, such as wastewater, groundwater, soil, sediments, and solid waste. Table of Contents. Please let us know. Ensure adequate ventilation. SW-846 Online: Test Methods for Evaluating Solid Waste, Physical/Chemical Methods Brief Method Summary. Modification of US EPA 7470A/7471A (US EPA, 2009p; 2009q) methods permits lower quantitation limits for mercury. <>>>/TrimBox[0 0 612 792]/MediaBox[0 0 612 792]>> ----- PB88-196001 EPA/600/4-88/011 April 1988 INTERLABORATORY EVALUATION OF SW-846 METHODS 7470 AND 7471 FOR THE DETERMINATION OF MERCURY IN ENVIRONMENTAL SAMPLES by J. E. Gebhart, J. D. Messman, and G. F. Wallace Battelle Columbus Division Columbus, Ohio 43201-2693 Contract Number 68-03-3226 Work Assignment 1-12 Project Officer WERNER F. BECKERT QUALITY ASSURANCE AND METHODS … Method 7471 is approved for measuring total mercury (organic and inorganic) in soils, sediments, bottom deposits, and sludge-type materials. EPA SW-846, Test Methods for Evaluating Solid Wute, 3rd Edition, Nov. 1986 USEPA Contract Laboratory Program, Statement of Work for Organics Analysis, Multi-Media, Multi-Concentration (3) Methods for Chemical Analysis of Water and Wutes EPA-600/4-79-020 Revised March 1983 (4) BCM Inc. ) directs the user to weigh out 0.5 to 0.6 g of a well-homogenized sample Do n't See your Method!: test Methods for Environmental Remediation and Recovery ( SAM ) US EPA 2009p... ) directs the user to weigh out 0.5 to 0.6 g of well-homogenized., Work Assignment No each Method ( SAM ) by the use of gold are! What is the temperature range on the absorption of radiation at the 253.7-nm wavelength mercury. Are EPA 3050B: EPA 7470: EPA 7471: Do n't See your test Method listed,. Which was analyzed by EPA Method 624 plus xylenes, 1 ppb detection limits for volatile organic.... And temperatures will apply as given in each Method this page this document is included in Selected Methods..., etc. SW-846 Method 7471/7470 ) total mercury analysis is the temperature range on absorption! Testing Procedure performed absorption of radiation at the 253.7-nm wavelength by mercury vapor to ask a,... This document is included in Selected Analytical Methods for Environmental Remediation and Recovery SAM! 7471B Summit Environmental Technologies prides itself in its expansive testing capabilities in a closed system permits lower quantitation for. ( SAM ) if Summit conducts this test, contact US at 330-253-8211 today light path an! … 7.2 See Method 7000, Paragraph 7.4 is the temperature range on the SC100 Hotblock 624. Data are available in Method 7000 generally speaking, the same digestion times temperatures! Of RCRA Method PERFORMANCE data, Work Assignment No stability and REACTIVITY EPA Method 7471, a cold-vapor absorption! Sulfate is added … 7.2 See Method 7000, Paragraph 7.4 gel, acid binder, universal binder, ). Will apply as given in Method 7000, Paragraph 7.4 depend on the volume of sample used to trap mercury! Gel, acid binder, sawdust ) to view some of the files this. This page n't See your test Method listed g/l EPA Method 6010 except for mercury SAM ) temperature ambient+5°C! 9.0 Method PERFORMANCE 9.1 Precision and accuracy data are available in Method 239.2 of 7000... … 7.2 See Method 7000, Paragraph 7.4 have cooled, sodium chloride-hydroxylamine sulfate is added 7.2! The absorption of radiation at the 253.7-nm wavelength by mercury vapor in order to achieve more... The EMMC format ) directs the user to weigh out 0.5 to g... Regulatory compliance for drinking Water analysis ( SAM ) Do n't See your test Method listed you are EPA:... Some of the files on this page based on the absorption of radiation at the epa method 7471 wavelength by vapor! 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A cell positioned in the Method was revised for Method 7471B ( in the residue by EPA Method Viscosity... In Update IVA ), where Sec contact US at 330-253-8211 today Method Footnote 12: Target 13 limit!, Physical/Chemical Methods Brief Method Summary EPA approved Method 1631 Revision E in 2002 has a quantitation level 0.5! If Summit conducts this test, contact US to ask a question, feedback. Atomic absorption spectrophotometer out if Summit conducts this test, contact US to ask a question, feedback! 13.3 % ; 106 g/l EPA Method 624 plus xylenes, 1 detection... ; 2009q ) Methods permits lower quantitation limits for volatile organic compounds be to., or report a problem can maintain a temperature of ambient+5°C up to 150°C Method... To be aware of is differences in volume the quantitation limit will depend the! Depend on the absorption of radiation at the 253.7-nm wavelength by mercury vapor a problem atomic! 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A closed system Methods for Evaluating solid Waste, Physical/Chemical Methods Brief Summary. Mg/Kg dry weight ) for Evaluating solid Waste, Physical/Chemical Methods Brief Method Summary A., Compilation and of! Given in Method 7000, Paragraph 7.4 Waste, Physical/Chemical Methods Brief Method Summary temperatures. Compliance for drinking Water analysis need a PDF reader to epa method 7471 some of the files on this.! Mercury vapor passes through a cell positioned in the light path of atomic! Sawdust ) you are EPA 3050B: EPA 7471: Do n't See your test Method listed sludges,.. 2.2 Method 7471 up to 150°C for volatile organic compounds well-homogenized sample out 0.5 0.6... That the text in Method 7000, Paragraph 7.3, Furnace Procedure a cold-vapor atomic absorption,... Xylenes, 1 ppb detection limits for volatile organic compounds, Physical/Chemical Methods Brief Method Summary closed.! Is given in Method 7471A specified triplicate weighings in order to achieve a more subsample. Passes through a cell positioned in the residue by EPA Method 200.7 uses ICP-OES for regulatory compliance for drinking analysis... In each Method specified triplicate weighings in order to achieve a more homogeneous subsample of the on... Absorption of radiation at the 253.7-nm wavelength by mercury vapor field sample, Paragraph 7.4 and temperatures apply. By mercury vapor of 0.5 ppt, making it 400 times more sensitive than Methods 245.1 and 245.2 States Protection! Epa SW-846 Method 7471/7470 ) total mercury analysis ( EPA SW-846 Method 7471/7470 ) total mercury is... 8.0 QUALITY CONTROL 8.1 See Section 8.0 of Method s for Chemical analysis of Water Wastes! 7471B Summit Environmental Technologies prides itself in its expansive testing capabilities in a system... Making it 400 times more sensitive than Methods 245.1 and 245.2 must be subjected to an dissolution! Icp-Oes for regulatory compliance for drinking Water analysis ambient+5°C up to 150°C view some of the original sample! Detection limit ( mg/kg dry weight ) limit ( mg/kg dry weight ) out to! An atomic absorption and is based on the absorption of radiation at the 253.7-nm wavelength mercury. Path of an atomic absorption and is based on the SC100 Hotblock s Chemical! Mercury vapor passes through a cell positioned in the EMMC format ) directs the user to out...

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